The only cryogenic gas concentrator engineered to recover trace non-volatile compounds from liquid CO₂ with precision and repeatability.

In beverage-grade carbon dioxide and other cryogenic gases, trace contamination by non-volatile compounds (NVOCs)—such as glycols, oils, and heavy hydrocarbons—can compromise product quality and safety. Conventional gas chromatographic sampling fails in these applications because vaporizing the CO₂ matrix at high temperatures causes unpredictable flashing, resulting in non-repeatable data.
The Wasson-ECE NVOC addresses this challenge by selectively vaporizing low-boiling matrices (like CO₂) while concentrating high-boiling contaminants. This enables accurate and reproducible quantification of trace NVOCs using standard GC or GC/MS systems.
Specification
Concentration of non-volatile organics from liquid CO₂ for GC injection
-18 to 65°C (0 to 149°F)
1000 psig
400 psig
65 psig
240 VAC, 50/60 Hz, 10A Max
55 psig dry air or nitrogen
Built-in 5 µm NUPRO FW filter (user-replaceable)
Digital totalizer (mL or g units)
Wasson-ECE Instrumentation has over 35 years of expertise in gas chromatography and process analytical systems. The NVOC was engineered from decades of experience in gas-phase and cryogenic analysis for the beverage, petrochemical, and environmental industries, ensuring robust design, reliability, and analytical integrity.
- Selective Vaporization Technology: The NVOC performs vaporization inside a capillary column section, where CO₂ vaporizes and vents while non-volatile residues are trapped. A solvent flush then dissolves and concentrates the residue for syringe injection into the GC—enabling direct analysis of compounds previously undetectable via gas-phase injection.
- Precise Flow and Mass Control: A digital flow totalizer measures total vaporized CO₂ mass and volume, ensuring accurate concentration calculations and repeatable sampling.
- Fully Integrated Analytical Workflow: The NVOC interfaces directly with standard gas chromatographs, providing a complete workflow—from sample introduction to quantification—without specialized hardware or modification to the GC system.
In beverage-grade carbon dioxide and other cryogenic gases, trace contamination by non-volatile compounds (NVOCs)—such as glycols, oils, and heavy hydrocarbons—can compromise product quality and safety. Conventional gas chromatographic sampling fails in these applications because vaporizing the CO₂ matrix at high temperatures causes unpredictable flashing, resulting in non-repeatable data.
The Wasson-ECE NVOC addresses this challenge by selectively vaporizing low-boiling matrices (like CO₂) while concentrating high-boiling contaminants. This enables accurate and reproducible quantification of trace NVOCs using standard GC or GC/MS systems.
Specification
Concentration of non-volatile organics from liquid CO₂ for GC injection
-18 to 65°C (0 to 149°F)
1000 psig
400 psig
65 psig
240 VAC, 50/60 Hz, 10A Max
55 psig dry air or nitrogen
Built-in 5 µm NUPRO FW filter (user-replaceable)
Digital totalizer (mL or g units)
Wasson-ECE Instrumentation has over 35 years of expertise in gas chromatography and process analytical systems. The NVOC was engineered from decades of experience in gas-phase and cryogenic analysis for the beverage, petrochemical, and environmental industries, ensuring robust design, reliability, and analytical integrity.
- Selective Vaporization Technology: The NVOC performs vaporization inside a capillary column section, where CO₂ vaporizes and vents while non-volatile residues are trapped. A solvent flush then dissolves and concentrates the residue for syringe injection into the GC—enabling direct analysis of compounds previously undetectable via gas-phase injection.
- Precise Flow and Mass Control: A digital flow totalizer measures total vaporized CO₂ mass and volume, ensuring accurate concentration calculations and repeatable sampling.
- Fully Integrated Analytical Workflow: The NVOC interfaces directly with standard gas chromatographs, providing a complete workflow—from sample introduction to quantification—without specialized hardware or modification to the GC system.
The NVOC’s unique vaporization and solvent recovery method enables:
- Recovery efficiency of >95% for glycols and C₁₀+ hydrocarbons in CO₂ matrices.
- Reproducibility of <5% RSD for replicate samples.
- Quantitative trace detection down to low ppm levels, depending on GC/MS configuration.
- Dimensions: Bench-top enclosure (approx. 18" W × 12" H × 20" D)
- Construction: 316L stainless steel, chemically inert wetted surfaces
- Valve Type: 6-port pneumatic valve (A60 or AT60 actuator)
- Tubing Connections: 1/8" Swagelok™ bulkheads (sample/gas) and 1/16" unions (solvent lines)
- Capillary Restrictor: 3 m × 0.10 mm stainless steel capillary
- Filtration: 5 µm NUPRO FW in-line filter
- Sensors: Digital mass/flow totalizer for vaporized CO₂ measurement
- Power: 240 VAC, 50/60 Hz, 10A
- Pneumatics:
- 55 psig dry air or nitrogen (actuation gas)
- 400 psig purge gas (zero-grade N₂ or air)
- Ventilation: Proper vent line or fume hood required for CO₂ and solvent exhaust
- Environment: 0–65°C operation, indoor laboratory or analytical enclosure
- Solvents: Compatible with methanol, acetone, and other GC-grade solvents
The NVOC captures trace non-volatile compounds by:
- Introducing a pressurized liquid CO₂ sample into a restrictive capillary vaporization zone.
- Allowing CO₂ to vaporize and vent while non-volatile residues deposit inside the capillary.
- Forcing a solvent flush through the capillary to dissolve and recover the residue.
- Injecting the solvent fraction directly into a GC or GC/MS for quantification.
This controlled process provides repeatable concentration factors, enabling direct calculation of actual NVOC concentration in liquid CO₂.
Wasson-ECE Instrumentation
101 Rome Ct., Fort Collins, Colorado USA 80524
Phone: +1 (970) 221-9179
Fax: +1 (970) 221-9364
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